PMID- 36728597
OWN - NLM
STAT- MEDLINE
DCOM- 20230321
LR  - 20230321
IS  - 1532-4109 (Electronic)
IS  - 0360-1234 (Linking)
VI  - 58
IP  - 2
DP  - 2023
TI  - Simultaneous detection of four pesticides in agricultural products by a modified 
      QuEChERS method and LC-MS/MS.
PG  - 150-157
LID - 10.1080/03601234.2023.2173926 [doi]
AB  - A modified QuEChERS pretreatment method and LC-MS/MS technique were performed to 
      simultaneously determine four pesticide (Hexachlorophene, Dinex, Dinosam, 
      Dinoterb) residues in agricultural products. Through the optimization of LC-MS/MS 
      detection parameters in SIM mode, the optimal instrument conditions are obtained. 
      The modified QuEChERS method was used to pretreat the samples. Solid phase 
      extractants PSA, C18 and GCB were used for sample purification. The research 
      results showed that the correlation coefficients of the four pesticides were all 
      greater than 0.991, which had a good linear relationship. The limits of 
      quantitation (LOQ) of the four pesticides were 0.05-0.56 mug/kg. The recoveries 
      were 70.51-113.20% with relative standard deviations (RSDS) of 1.6-11.2%. The 
      developed method can provide reliable data support for the subsequent 
      simultaneous detection of these four pesticides.
FAU - Zheng, Kunming
AU  - Zheng K
AD  - Fujian CCIC-Fairreach Food Safety Testing Co., Ltd, Fuzhou, China.
FAU - Guo, Yuanjun
AU  - Guo Y
AD  - College of Biological and Environmental Engineering, Jingdezhen University, 
      Jingdezhen, China.
FAU - Hu, Xunke
AU  - Hu X
AD  - The Second People's Hospital of Jingdezhen, Jingdezhen, China.
FAU - Yu, Yaping
AU  - Yu Y
AD  - The Second People's Hospital of Jingdezhen, Jingdezhen, China.
FAU - Chen, Jinxing
AU  - Chen J
AD  - Fujian CCIC-Fairreach Food Safety Testing Co., Ltd, Fuzhou, China.
FAU - Su, Jianfeng
AU  - Su J
AD  - Fujian CCIC-Fairreach Food Safety Testing Co., Ltd, Fuzhou, China.
FAU - Lian, Wenhao
AU  - Lian W
AD  - Fujian CCIC-Fairreach Food Safety Testing Co., Ltd, Fuzhou, China.
FAU - Wu, Xiaoping
AU  - Wu X
AD  - Fujian CCIC-Fairreach Food Safety Testing Co., Ltd, Fuzhou, China.
FAU - Meng, Xingang
AU  - Meng X
AUID- ORCID: 0000-0001-8036-3714
AD  - College of Biological and Environmental Engineering, Jingdezhen University, 
      Jingdezhen, China.
LA  - eng
PT  - Journal Article
DEP - 20230202
PL  - England
TA  - J Environ Sci Health B
JT  - Journal of environmental science and health. Part. B, Pesticides, food 
      contaminants, and agricultural wastes
JID - 7607167
RN  - 0 (Pesticides)
RN  - 0 (Pesticide Residues)
SB  - IM
MH  - *Pesticides/analysis
MH  - Chromatography, Liquid/methods
MH  - *Pesticide Residues/analysis
MH  - Tandem Mass Spectrometry/methods
OTO - NOTNLM
OT  - LC-MS/MS
OT  - Pesticides
OT  - QuEChERS
OT  - agricultural products
OT  - detection
EDAT- 2023/02/03 06:00
MHDA- 2023/03/22 06:00
CRDT- 2023/02/02 09:23
PHST- 2023/02/03 06:00 [pubmed]
PHST- 2023/03/22 06:00 [medline]
PHST- 2023/02/02 09:23 [entrez]
AID - 10.1080/03601234.2023.2173926 [doi]
PST - ppublish
SO  - J Environ Sci Health B. 2023;58(2):150-157. doi: 10.1080/03601234.2023.2173926. 
      Epub 2023 Feb 2.