PMID- 36744283
OWN - NLM
STAT- PubMed-not-MEDLINE
LR  - 20230207
IS  - 2046-2069 (Electronic)
IS  - 2046-2069 (Linking)
VI  - 13
IP  - 7
DP  - 2023 Jan 31
TI  - Efficient analyses of triazole fungicides in water, honey and soy milk samples by 
      popping candy-generated CO(2) and sugaring-out-assisted supramolecular 
      solvent-based microextraction prior to HPLC determinations.
PG  - 4195-4201
LID - 10.1039/d2ra06560f [doi]
AB  - An enrichment method, namely popping candy-generated CO(2) and 
      sugaring-out-assisted supramolecular solvent-based microextraction (PGS-SUPRA), 
      was investigated for the determination of triazole fungicide residues in water, 
      honey and soy milk samples. The extraction process was carried out by adding 
      popping candies into a centrifuge tube. Consequently, rapid dispersion and mass 
      transfer of extractants can be achieved without using dispersants and auxiliary 
      devices, and therefore, the extraction efficiency increased. The extraction 
      parameters affecting the efficiency of the developed method were investigated. 
      The presented method was then analysed by high-performance liquid chromatography. 
      Under the selected condition, the wide linearity of triazole fungicides after 
      preconcentration by the proposed microextraction method ranged from 30 to 1000 mug 
      L(-1) for triadimefon and from 90 to 1000 mug L(-1) for myclobutanil, tebuconazole 
      and hexaconazole, with a coefficient for determination (R (2)) greater than 
      0.992. The limits of detection (LODs) and limits of quantitation (LOQs) were in 
      the range of 10-30 mug L(-1) and 30-90 mug L(-1), respectively. The precisions were 
      assessed from the relative standard deviations (RSDs) of the retention time and 
      peak area obtained from intra- (n = 3) and inter-day (n = 3 x 5) experiments, and 
      were greater than 1.66% and 13.52%, respectively. Moreover, the proposed method 
      provided high enhancement factors (EnFs) ranging from 14 to 51 folds. This 
      technique has been prosperously applied for the extraction of fungicide residues 
      in water, honey and soy milk samples with a recovery within the range of 60-114%. 
      Overall, the developed method was found to be advantageous as compared with other 
      sample preparation methods.
CI  - This journal is (c) The Royal Society of Chemistry.
FAU - Jaroensan, Jedsada
AU  - Jaroensan J
AD  - Creative Chemistry and Innovation Research Unit, Department of Chemistry and 
      Center of Excellence for Innovation in Chemistry, Faculty of Science, 
      Mahasarakham University Maha Sarakham 44150 Thailand jitlada.v@msu.ac.th +66 4375 
      4246 +66 4375 4246.
FAU - Khiaophong, Wannipha
AU  - Khiaophong W
AD  - Creative Chemistry and Innovation Research Unit, Department of Chemistry and 
      Center of Excellence for Innovation in Chemistry, Faculty of Science, 
      Mahasarakham University Maha Sarakham 44150 Thailand jitlada.v@msu.ac.th +66 4375 
      4246 +66 4375 4246.
FAU - Kachangoon, Rawikan
AU  - Kachangoon R
AD  - Creative Chemistry and Innovation Research Unit, Department of Chemistry and 
      Center of Excellence for Innovation in Chemistry, Faculty of Science, 
      Mahasarakham University Maha Sarakham 44150 Thailand jitlada.v@msu.ac.th +66 4375 
      4246 +66 4375 4246.
FAU - Vichapong, Jitlada
AU  - Vichapong J
AUID- ORCID: 0000-0003-4637-4465
AD  - Creative Chemistry and Innovation Research Unit, Department of Chemistry and 
      Center of Excellence for Innovation in Chemistry, Faculty of Science, 
      Mahasarakham University Maha Sarakham 44150 Thailand jitlada.v@msu.ac.th +66 4375 
      4246 +66 4375 4246.
AD  - Multidisciplinary Research Unit of Pure and Applied Chemistry (MRUPAC), 
      Department of Chemistry and Center of Excellent for Innovation in Chemistry, 
      Faculty of Science, Mahasarakham University Maha Sarakham 44150 Thailand.
LA  - eng
PT  - Journal Article
DEP - 20230131
PL  - England
TA  - RSC Adv
JT  - RSC advances
JID - 101581657
PMC - PMC9890668
COIS- There are no conflicts to declare.
EDAT- 2023/02/07 06:00
MHDA- 2023/02/07 06:01
PMCR- 2023/01/31
CRDT- 2023/02/06 04:07
PHST- 2022/10/18 00:00 [received]
PHST- 2023/01/18 00:00 [accepted]
PHST- 2023/02/06 04:07 [entrez]
PHST- 2023/02/07 06:00 [pubmed]
PHST- 2023/02/07 06:01 [medline]
PHST- 2023/01/31 00:00 [pmc-release]
AID - d2ra06560f [pii]
AID - 10.1039/d2ra06560f [doi]
PST - epublish
SO  - RSC Adv. 2023 Jan 31;13(7):4195-4201. doi: 10.1039/d2ra06560f. eCollection 2023 
      Jan 31.