PMID- 37081364
OWN - NLM
STAT- MEDLINE
DCOM- 20230424
LR  - 20230424
IS  - 1573-2959 (Electronic)
IS  - 0167-6369 (Linking)
VI  - 195
IP  - 5
DP  - 2023 Apr 20
TI  - Development of QuEChERS coupled with UHPLC-MS/MS for simultaneous determination 
      of eight neonicotinoid pesticides in breast milk.
PG  - 597
LID - 10.1007/s10661-023-11185-x [doi]
AB  - A speedy and hypersensitive method was built to detect eight neonicotinoid 
      insecticides (neonics) in breast milk by ultrahigh-performance liquid 
      chromatography-tandem mass spectrometry (UHPLC-MS/MS). The breast milk was 
      extracted with a mixture of acetonitrile and water and purified with primary 
      secondary amine (PSA) and C18. The recovery of the method ranged from 74.3 to 
      105.9% with relative standard deviations (RSDs) of less than 10%, and the limit 
      of detection ranged from 0.05 to 0.18 ng/mL. Among 32 samples obtained from women 
      1 month postpartum, thiamethoxam and imidacloprid were the most frequently 
      detected neonics. Moreover, thiacloprid and imidaclothiz were not detected in any 
      samples. The concentrations of neonics in breast milk ranged from 1.90 to 
      149.95 ng/mL. Considering the toxic effects on mammals and even humans, infants 
      who are exposed to neonics through ingestion of breast milk should receive 
      extensive attention in future studies.
CI  - (c) 2023. The Author(s), under exclusive licence to Springer Nature Switzerland AG.
FAU - Ying, Zeteng
AU  - Ying Z
AD  - Key Laboratory of Microbial Technology for Industrial Pollution Control of 
      Zhejiang Province, College of Environment, Zhejiang University of Technology, 
      Hangzhou, Zhejiang, 310032, People's Republic of China.
FAU - Fu, Lili
AU  - Fu L
AD  - Key Laboratory of Microbial Technology for Industrial Pollution Control of 
      Zhejiang Province, College of Environment, Zhejiang University of Technology, 
      Hangzhou, Zhejiang, 310032, People's Republic of China.
FAU - Gu, Sijia
AU  - Gu S
AD  - Key Laboratory of Microbial Technology for Industrial Pollution Control of 
      Zhejiang Province, College of Environment, Zhejiang University of Technology, 
      Hangzhou, Zhejiang, 310032, People's Republic of China.
FAU - Wang, Yan
AU  - Wang Y
AD  - Key Laboratory of Microbial Technology for Industrial Pollution Control of 
      Zhejiang Province, College of Environment, Zhejiang University of Technology, 
      Hangzhou, Zhejiang, 310032, People's Republic of China.
FAU - Mo, Xunjie
AU  - Mo X
AD  - Key Laboratory of Microbial Technology for Industrial Pollution Control of 
      Zhejiang Province, College of Environment, Zhejiang University of Technology, 
      Hangzhou, Zhejiang, 310032, People's Republic of China.
FAU - Tang, Tao
AU  - Tang T
AD  - State Key Laboratory for Quality and Safety of Agro-Products, Key Laboratory for 
      Pesticide Residue Detection of Ministry of Agriculture and Rural Affairs, 
      Institute of Quality and Standard for Agro-Products, Zhejiang Academy of 
      Agricultural Sciences, Hangzhou, Zhejiang, 310021, People's Republic of China.
FAU - Jin, Hangbiao
AU  - Jin H
AD  - Key Laboratory of Microbial Technology for Industrial Pollution Control of 
      Zhejiang Province, College of Environment, Zhejiang University of Technology, 
      Hangzhou, Zhejiang, 310032, People's Republic of China.
FAU - Zhang, Quan
AU  - Zhang Q
AD  - Key Laboratory of Microbial Technology for Industrial Pollution Control of 
      Zhejiang Province, College of Environment, Zhejiang University of Technology, 
      Hangzhou, Zhejiang, 310032, People's Republic of China. quanzhang@zjut.edu.cn.
LA  - eng
GR  - LR21B070001/the Zhejiang Provincial Natural Science Foundation of China/
GR  - 2021R403061/Zhejiang Provincial University Student Science and Technology 
      Innovation Activity Plan/
PT  - Journal Article
DEP - 20230420
PL  - Netherlands
TA  - Environ Monit Assess
JT  - Environmental monitoring and assessment
JID - 8508350
RN  - 0 (Pesticides)
RN  - 0 (Neonicotinoids)
RN  - 0 (Insecticides)
SB  - IM
MH  - Animals
MH  - Female
MH  - Humans
MH  - Chromatography, High Pressure Liquid/methods
MH  - Milk, Human/chemistry
MH  - Tandem Mass Spectrometry/methods
MH  - *Pesticides/analysis
MH  - Environmental Monitoring
MH  - Neonicotinoids/analysis
MH  - *Insecticides/analysis
MH  - Mammals
OTO - NOTNLM
OT  - Breast milk
OT  - Infants
OT  - Neonicotinoids
OT  - Pretreatment
OT  - UHPLC-MS/MS
EDAT- 2023/04/21 00:42
MHDA- 2023/04/24 06:42
CRDT- 2023/04/20 23:33
PHST- 2022/09/24 00:00 [received]
PHST- 2023/04/01 00:00 [accepted]
PHST- 2023/04/24 06:42 [medline]
PHST- 2023/04/21 00:42 [pubmed]
PHST- 2023/04/20 23:33 [entrez]
AID - 10.1007/s10661-023-11185-x [pii]
AID - 10.1007/s10661-023-11185-x [doi]
PST - epublish
SO  - Environ Monit Assess. 2023 Apr 20;195(5):597. doi: 10.1007/s10661-023-11185-x.