PMID- 37146852
OWN - NLM
STAT- MEDLINE
DCOM- 20230619
LR  - 20230619
IS  - 1879-0003 (Electronic)
IS  - 0141-8130 (Linking)
VI  - 242
IP  - Pt 2
DP  - 2023 Jul 1
TI  - Fractionation of depectinated sugar beet pulp into cellulose, hemicellulose, and 
      lignin with NaOH/urea/H(2)O and ionic liquid.
PG  - 124706
LID - S0141-8130(23)01600-8 [pii]
LID - 10.1016/j.ijbiomac.2023.124706 [doi]
AB  - This study proposes a novel and feasible dissolution and fractionation method of 
      depectinated sugar beet pulp (SBP) in NaOH/Urea/H(2)O, ionic liquid (IL) and 
      alkaline treatment processes. Interestingly, the complicated structure of SBP can 
      be treated with 30 % H(2)SO(4) to increase the dissolution rate. Scanning 
      electron microscope (SEM) analysis confirmed that the appearance of cellulose and 
      hemicellulose obtained by two methods were different. At the same time, two 
      lignin fractions showed irregular high-density clusters, which were composed of a 
      large number of submicron particles. The crystal structure of two cellulose 
      fractions changed from cellulose I to cellulose II. The thermal stability of 
      cellulose and lignin obtained by ionic liquid was slightly better than that 
      obtained by NaOH/urea/H(2)O. Results of Fourier transform infrared (FTIR) and 
      (13)C NMR showed that the chemical structures of SBP cellulose, hemicellulose and 
      lignin regenerated from NaOH/urea/H(2)O and ionic liquid were similar.
CI  - Copyright (c) 2023. Published by Elsevier B.V.
FAU - Liu, Qiang
AU  - Liu Q
AD  - School of Food Science and Engineering, South China University of Technology, 
      Guangzhou 510640, China.
FAU - Zhu, Siming
AU  - Zhu S
AD  - School of Food Science and Engineering, South China University of Technology, 
      Guangzhou 510640, China; Overseas Expertise Introduction Center for Discipline 
      Innovation of Food Nutrition and Human Health (111 Center), Guangzhou 510641, 
      China; Guangdong Province Key Laboratory for Green Processing of Natural Products 
      and Product Safety, Guangzhou 510641, China; College of Life and Geographic 
      Sciences, Kashi University, Kashi 844000, China. Electronic address: 
      lfsmzhu@scut.edu.cn.
LA  - eng
PT  - Journal Article
DEP - 20230503
PL  - Netherlands
TA  - Int J Biol Macromol
JT  - International journal of biological macromolecules
JID - 7909578
RN  - 9004-34-6 (Cellulose)
RN  - 9005-53-2 (Lignin)
RN  - 8024-50-8 (hemicellulose)
RN  - 0 (Ionic Liquids)
RN  - 55X04QC32I (Sodium Hydroxide)
RN  - 8W8T17847W (Urea)
RN  - 0 (Sugars)
SB  - IM
MH  - Cellulose/chemistry
MH  - Lignin/chemistry
MH  - *Ionic Liquids/chemistry
MH  - *Beta vulgaris
MH  - Sodium Hydroxide
MH  - Urea
MH  - Sugars
MH  - Hydrolysis
OTO - NOTNLM
OT  - Fractionation
OT  - Hemicellulose
OT  - Ionic liquid
OT  - Lignin
OT  - NaOH/urea
OT  - Regenerated cellulose
COIS- Declaration of competing interest The authors declare no competing financial 
      interest.
EDAT- 2023/05/06 09:42
MHDA- 2023/06/19 13:08
CRDT- 2023/05/05 19:27
PHST- 2023/01/03 00:00 [received]
PHST- 2023/04/02 00:00 [revised]
PHST- 2023/04/28 00:00 [accepted]
PHST- 2023/06/19 13:08 [medline]
PHST- 2023/05/06 09:42 [pubmed]
PHST- 2023/05/05 19:27 [entrez]
AID - S0141-8130(23)01600-8 [pii]
AID - 10.1016/j.ijbiomac.2023.124706 [doi]
PST - ppublish
SO  - Int J Biol Macromol. 2023 Jul 1;242(Pt 2):124706. doi: 
      10.1016/j.ijbiomac.2023.124706. Epub 2023 May 3.