PMID- 37241976
OWN - NLM
STAT- MEDLINE
DCOM- 20230529
LR  - 20230530
IS  - 1420-3049 (Electronic)
IS  - 1420-3049 (Linking)
VI  - 28
IP  - 10
DP  - 2023 May 22
TI  - Highly-Selective Analytical Strategy for 90 Pesticides and Metabolites Residues 
      in Fish and Shrimp Samples.
LID - 10.3390/molecules28104235 [doi]
LID - 4235
AB  - The analysis of pesticide residues in aquatic products is challenging due to low 
      residue levels and the complex matrix interference. In this study, we developed a 
      simple, fast method for the trace analysis of 90 pesticides and metabolites in 
      aquatic products. The analytes covered a wide polarity range with log Kow (log 
      octanol-water partition coefficient) ranging from -1.2 to 6.37. Grass carp 
      (Ctenopharyngodon idellus) and prawn (Penaeus chinensis) samples were chosen to 
      validate the quantification method. The samples were extracted by 0.2% 
      formic-acetonitrile, cleaned by solid-phase extraction (PRiME HLB), and analyzed 
      by high performance liquid chromatography-tandem mass spectrometry. The results 
      showed good linearities for the analytes and were observed in the range of 
      0.05-50 mug/L. The recoveries of the method were within 50.4-118.6%, with the 
      relative standard deviations being lower than 20%. The limits of quantifications 
      (LOQs) of the method were in the range of 0.05-5.0 mug/kg, which were superior to 
      values compared with other research. The developed method was applied to detect 
      pesticide residues in prawn samples from eastern coastal areas of China. Three 
      herbicide residues of diuron, prometryn, and atrazine were detected in prawn 
      samples. The method was sensitive and efficient, which is of significance in 
      expanding the screening scope and improving the quantitative analysis efficiency 
      in aquatic products.
FAU - Guo, Yage
AU  - Guo Y
AD  - State Key Laboratory for Biology of Plant Diseases and Insect Pests, Institute of 
      Plant Protection, Chinese Academy of Agricultural Sciences, Beijing 100193, 
      China.
FAU - Xie, Jun
AU  - Xie J
AD  - State Key Laboratory for Biology of Plant Diseases and Insect Pests, Institute of 
      Plant Protection, Chinese Academy of Agricultural Sciences, Beijing 100193, 
      China.
FAU - Dong, Fengshou
AU  - Dong F
AD  - State Key Laboratory for Biology of Plant Diseases and Insect Pests, Institute of 
      Plant Protection, Chinese Academy of Agricultural Sciences, Beijing 100193, 
      China.
FAU - Wu, Xiaohu
AU  - Wu X
AD  - State Key Laboratory for Biology of Plant Diseases and Insect Pests, Institute of 
      Plant Protection, Chinese Academy of Agricultural Sciences, Beijing 100193, 
      China.
FAU - Pan, Xinglu
AU  - Pan X
AD  - State Key Laboratory for Biology of Plant Diseases and Insect Pests, Institute of 
      Plant Protection, Chinese Academy of Agricultural Sciences, Beijing 100193, 
      China.
FAU - Liu, Xingang
AU  - Liu X
AD  - State Key Laboratory for Biology of Plant Diseases and Insect Pests, Institute of 
      Plant Protection, Chinese Academy of Agricultural Sciences, Beijing 100193, 
      China.
FAU - Zheng, Yongquan
AU  - Zheng Y
AD  - State Key Laboratory for Biology of Plant Diseases and Insect Pests, Institute of 
      Plant Protection, Chinese Academy of Agricultural Sciences, Beijing 100193, 
      China.
FAU - Zhang, Jie
AU  - Zhang J
AD  - Institute of Zoology, Chinese Academy of Sciences, Beijing 100101, China.
FAU - Xu, Jun
AU  - Xu J
AD  - State Key Laboratory for Biology of Plant Diseases and Insect Pests, Institute of 
      Plant Protection, Chinese Academy of Agricultural Sciences, Beijing 100193, 
      China.
LA  - eng
GR  - NSFC32072467/Nature Science Foundation of China/
PT  - Journal Article
DEP - 20230522
PL  - Switzerland
TA  - Molecules
JT  - Molecules (Basel, Switzerland)
JID - 100964009
RN  - 0 (Pesticides)
RN  - 0 (Pesticide Residues)
RN  - 0 (Herbicides)
SB  - IM
MH  - Animals
MH  - *Pesticides/analysis
MH  - *Pesticide Residues/analysis
MH  - Tandem Mass Spectrometry/methods
MH  - Chromatography, High Pressure Liquid/methods
MH  - *Herbicides/analysis
MH  - Fishes
MH  - Crustacea
MH  - Solid Phase Extraction/methods
PMC - PMC10222193
OTO - NOTNLM
OT  - HPLC-MS/MS
OT  - SPE
OT  - aquatic products
OT  - pesticide
OT  - residue
COIS- The authors declare that they have no known competing financial interest or 
      personal relationships that could have appeared to influence the work reported in 
      this paper.
EDAT- 2023/05/27 09:42
MHDA- 2023/05/29 06:42
PMCR- 2023/05/22
CRDT- 2023/05/27 01:25
PHST- 2023/04/26 00:00 [received]
PHST- 2023/05/14 00:00 [revised]
PHST- 2023/05/16 00:00 [accepted]
PHST- 2023/05/29 06:42 [medline]
PHST- 2023/05/27 09:42 [pubmed]
PHST- 2023/05/27 01:25 [entrez]
PHST- 2023/05/22 00:00 [pmc-release]
AID - molecules28104235 [pii]
AID - molecules-28-04235 [pii]
AID - 10.3390/molecules28104235 [doi]
PST - epublish
SO  - Molecules. 2023 May 22;28(10):4235. doi: 10.3390/molecules28104235.