PMID- 37334037 OWN - NLM STAT- PubMed-not-MEDLINE LR - 20230620 IS - 2424-8002 (Electronic) IS - 2424-7723 (Print) IS - 2424-8002 (Linking) VI - 9 IP - 4 DP - 2023 TI - Metrological characterization of porosity graded beta-Ti21S triply periodic minimal surface cellular structure manufactured by laser powder bed fusion. PG - 729 LID - 10.18063/ijb.729 [doi] LID - 729 AB - The design of a functionally graded porous structure (FGPS) for use in prosthetic devices is crucial for meeting both mechanical and biological requirements. One of the most commonly used cellular structures in FGPS is the triply periodic minimal surface (TPMS) structure due to its ability to be defined by implicit equations, which allows for smooth transitions between layers. This study evaluates the feasibility of using a novel beta-Ti21S alloy to fabricate TPMS-based FGPS. This beta titanium alloy exhibits low elastic modulus (53 GPa) and good mechanical properties in as-built condition. Two TPMS FGPSs with relative density gradients of 0.17, 0.34, 0.50, 0.66, and 0.83 and unit cell sizes of 2.5 mm and 4 mm were designed and fabricated using laser powder bed fusion (LPBF). The as-manufactured structures were analyzed using scanning electron microscopy (SEM) and X-ray micro-computed tomography (mu-CT), and the results were compared to the design. The analysis revealed that the pore size and ligament thickness were undersized by less than 5%. Compression tests showed that the stabilized elastic modulus was 4.1 GPa for the TPMS with a 2.5 mm unit cell size and 10.7 GPa for the TPMS with a 4 mm unit cell size. A finite element simulation was performed to predict the specimen's elastic properties, and a lumped model based on lattice homogenized properties was proposed and its limitations were explored. CI - Copyright: (c) 2023, Emanuelli L, De Biasi R, du Plessis A, et al. FAU - Emanuelli, Lorena AU - Emanuelli L AD - INSTM (Operative center: University of Trento), Trento, 38123, Italy. FAU - De Biasi, Raffaele AU - De Biasi R AD - Department of Industrial Engineering, University of Trento, Trento, Italy. FAU - Fu, Huijuan AU - Fu H AD - INSTM (Operative center: University of Trento), Trento, 38123, Italy. FAU - du Plessis, Anton AU - du Plessis A AD - Research Group 3D Innovation, Stellenbosch University, Stellenbosch, South Africa. AD - Object Research Systems, Montreal, Canada. FAU - Lora, Carlo AU - Lora C AD - SISMA SpA, Piovene Rocchette, Vicenza, Italy. FAU - Jam, Alireza AU - Jam A AD - Department of Industrial Engineering, University of Trento, Trento, Italy. FAU - Benedetti, Matteo AU - Benedetti M AD - Department of Industrial Engineering, University of Trento, Trento, Italy. FAU - Pellizzari, Massimo AU - Pellizzari M AD - Department of Industrial Engineering, University of Trento, Trento, Italy. LA - eng PT - Journal Article DEP - 20230407 PL - Singapore TA - Int J Bioprint JT - International journal of bioprinting JID - 101709763 PMC - PMC10272211 OTO - NOTNLM OT - Additive manufacturing OT - Functionally graded porous structures OT - Laser powder bed fusion OT - Metrological characterization OT - Skeletal-based triply periodic minimal surface structure OT - Ti-21S COIS- The authors declare that they have no known financial interests or personal relationships that could have appeared to influence the work reported in this paper. Alireza Jam is currently with the National Center for Additive Manufacturing Excellence (NCAME) at Auburn University. EDAT- 2023/06/19 06:41 MHDA- 2023/06/19 06:42 PMCR- 2023/04/07 CRDT- 2023/06/19 03:00 PHST- 2023/01/09 00:00 [received] PHST- 2023/02/28 00:00 [accepted] PHST- 2023/06/19 06:42 [medline] PHST- 2023/06/19 06:41 [pubmed] PHST- 2023/06/19 03:00 [entrez] PHST- 2023/04/07 00:00 [pmc-release] AID - IJB-9-4-729 [pii] AID - 10.18063/ijb.729 [doi] PST - epublish SO - Int J Bioprint. 2023 Apr 7;9(4):729. doi: 10.18063/ijb.729. eCollection 2023.