PMID- 38139968 OWN - NLM STAT- PubMed-not-MEDLINE LR - 20231225 IS - 2073-4360 (Electronic) IS - 2073-4360 (Linking) VI - 15 IP - 24 DP - 2023 Dec 15 TI - High-Density Polyethylene/Carbon Black Composites in Material Extrusion Additive Manufacturing: Conductivity, Thermal, Rheological, and Mechanical Responses. LID - 10.3390/polym15244717 [doi] LID - 4717 AB - High-density polyethylene polymer (HDPE) and carbon black (CB) were utilized to create HDPE/CB composites with different filler concentrations (0.0, 2.0, 4.0, 6.0, 8.0, 10.0, 16.0, 20.0, and 24.0 wt.%). The composites were extruded into filaments, which were then utilized to fabricate 3D-printed specimens with the material extrusion (MEX) method, suitable for a variety of standard mechanical tests. The electrical conductivity was investigated. Furthermore, thermogravimetric analysis and differential scanning calorimetry were carried out for all the HDPE/CB composites and pure HDPE. Scanning electron microscopy in different magnifications was performed on the specimens' fracture and side surfaces to investigate the morphological characteristics. Rheological tests and Raman spectroscopy were also performed. Eleven different tests in total were performed to fully characterize the composites and reveal connections between their various properties. HDPE/CB 20.0 wt.% showed the greatest reinforcement results in relation to pure HDPE. Such composites are novel in the MEX 3D printing method. The addition of the CB filler greatly enhanced the performance of the popular HDPE polymer, expanding its applications. FAU - Vidakis, Nectarios AU - Vidakis N AD - Department of Mechanical Engineering, Hellenic Mediterranean University, 71410 Heraklion, Greece. FAU - Petousis, Markos AU - Petousis M AUID- ORCID: 0000-0003-1312-7898 AD - Department of Mechanical Engineering, Hellenic Mediterranean University, 71410 Heraklion, Greece. FAU - Michailidis, Nikolaos AU - Michailidis N AUID- ORCID: 0000-0002-4291-5327 AD - Physical Metallurgy Laboratory, Mechanical Engineering Department, School of Engineering, Aristotle University of Thessaloniki, 54124 Thessaloniki, Greece. AD - Centre for Research & Development of Advanced Materials (CERDAM), Center for Interdisciplinary Research and Innovation, Balkan Centre, Building B', 10th km Thessaloniki-Thermi Road, 57001 Thessaloniki, Greece. FAU - Mountakis, Nikolaos AU - Mountakis N AUID- ORCID: 0000-0003-4509-8753 AD - Department of Mechanical Engineering, Hellenic Mediterranean University, 71410 Heraklion, Greece. FAU - Argyros, Apostolos AU - Argyros A AUID- ORCID: 0000-0002-7982-7742 AD - Physical Metallurgy Laboratory, Mechanical Engineering Department, School of Engineering, Aristotle University of Thessaloniki, 54124 Thessaloniki, Greece. AD - Centre for Research & Development of Advanced Materials (CERDAM), Center for Interdisciplinary Research and Innovation, Balkan Centre, Building B', 10th km Thessaloniki-Thermi Road, 57001 Thessaloniki, Greece. FAU - Spiridaki, Mariza AU - Spiridaki M AD - Department of Mechanical Engineering, Hellenic Mediterranean University, 71410 Heraklion, Greece. FAU - Moutsopoulou, Amalia AU - Moutsopoulou A AD - Department of Mechanical Engineering, Hellenic Mediterranean University, 71410 Heraklion, Greece. FAU - Papadakis, Vassilis AU - Papadakis V AUID- ORCID: 0000-0003-3188-4577 AD - Department of Industrial Design and Production Engineering, University of West Attica, 12244 Athens, Greece. AD - Institute of Electronic Structure and Laser, Foundation for Research and Technology-Hellas, N. Plastira 100m, 70013 Heraklion, Greece. FAU - Charitidis, Costas AU - Charitidis C AUID- ORCID: 0000-0003-1367-7603 AD - Department of Materials Science and Engineering, School of Chemical Engineering NTUA, National Technical University, Iroon Polytechneiou 9, Zografou, 15780 Athens, Greece. LA - eng PT - Journal Article DEP - 20231215 PL - Switzerland TA - Polymers (Basel) JT - Polymers JID - 101545357 PMC - PMC10747577 OTO - NOTNLM OT - 3D printing OT - additive manufacturing OT - carbon black OT - composites OT - electrical conductivity OT - high-density polyethylene OT - material extrusion OT - mechanical properties OT - melt flow index COIS- The authors declare no conflict of interest. EDAT- 2023/12/23 12:43 MHDA- 2023/12/23 12:44 PMCR- 2023/12/15 CRDT- 2023/12/23 01:25 PHST- 2023/11/24 00:00 [received] PHST- 2023/12/09 00:00 [revised] PHST- 2023/12/13 00:00 [accepted] PHST- 2023/12/23 12:44 [medline] PHST- 2023/12/23 12:43 [pubmed] PHST- 2023/12/23 01:25 [entrez] PHST- 2023/12/15 00:00 [pmc-release] AID - polym15244717 [pii] AID - polymers-15-04717 [pii] AID - 10.3390/polym15244717 [doi] PST - epublish SO - Polymers (Basel). 2023 Dec 15;15(24):4717. doi: 10.3390/polym15244717.