PMID- 38296128 OWN - NLM STAT- MEDLINE DCOM- 20240313 LR - 20240313 IS - 1879-0003 (Electronic) IS - 0141-8130 (Linking) VI - 261 IP - Pt 2 DP - 2024 Mar TI - Preparation and characterization of sodium caseinate-apricot tree gum/gum Arabic nanocomplex for encapsulation of conjugated linoleic acid (CLA). PG - 129773 LID - S0141-8130(24)00576-2 [pii] LID - 10.1016/j.ijbiomac.2024.129773 [doi] AB - Nanocomplexes (NCs) were formed through electrostatic complexation theory using Na-caseinate (NaCa), gum Arabic (GA), and Prunus armeniaca L. gum exudates (PAGE), aimed to encapsulate Conjugated linoleic acid (CLA). Encapsulation was optimized using NaCa (0.1 %-0.5 %), GA/PAGE (0.1 %-0.9 %) and CLA (1 %-5 %), and central composite design (CCD) was employed for numerical optimization. The optimum conditions for NC containing GA (NCGA) were 0.336 %, 0.437 %, and 3.10 % and for NC containing PAGE (NCPAGE) were 0.403 %, 0.730 %, and 4.177 %, of NaCa, GA/PAGE, and CLA, respectively. EE and particle size were 92.46 % and 52.89 nm for NCGA while 88.23 % and 54.76 nm for NCPAGE, respectively. Fourier transform infrared spectroscopy (FTIR) indicated that CLA was physically entrapped. Scanning electron microscopy (SEM) and transmission electron microscopy (TEM) confirmed the electrostatic complex formation. The elastic modulus was predominant for NCGA and NCPAGE dispersions while the complex viscosity of NCPAGE suspension was slightly higher than that of NCGA. The CLA in NCGA-CLA and NCPAGE-CLA exhibited higher oxidative stability than free CLA during 30 days of storage without a significant difference between the results of CLA oxidative stability tests obtained for NCs. Consequently, NCPAGE and NCGA could be applied for the entrapment and protection of nutraceuticals in the food industry. CI - Copyright (c) 2024. Published by Elsevier B.V. FAU - Gohari, Alireza Saeed AU - Gohari AS AD - Department of Food Science and Technology, Faculty of Agriculture, Varamin-Pishva Branch, Islamic Azad University, Varamin, Iran. FAU - Nateghi, Leila AU - Nateghi L AD - Department of Food Science and Technology, Faculty of Agriculture, Varamin-Pishva Branch, Islamic Azad University, Varamin, Iran. Electronic address: leylanateghi@iauvaramin.ac.ir. FAU - Rashidi, Ladan AU - Rashidi L AD - Research Center of Food Technology and Agricultural Products, Standard Research Institute (SRI), P.O. Box 31745-139, Karaj, Iran. Electronic address: l.rashidi@standard.ac.ir. FAU - Berenji, Shila AU - Berenji S AD - Department of Food Science and Technology, Faculty of Agriculture, Varamin-Pishva Branch, Islamic Azad University, Varamin, Iran. LA - eng PT - Journal Article DEP - 20240201 PL - Netherlands TA - Int J Biol Macromol JT - International journal of biological macromolecules JID - 7909578 RN - 9000-01-5 (Gum Arabic) RN - 0 (Caseins) RN - 0 (Linoleic Acids, Conjugated) SB - IM MH - Gum Arabic/chemistry MH - *Prunus armeniaca MH - Caseins/chemistry MH - *Linoleic Acids, Conjugated MH - Particle Size OTO - NOTNLM OT - Conjugated linoleic acid (CLA) OT - Gum Arabic (GA) OT - Nanocomplex (NC) OT - Prunus armeniaca L. gum exudates OT - Sodium caseinate COIS- Declaration of competing interest All authors have no conflicts of interest to declare. EDAT- 2024/02/01 00:42 MHDA- 2024/03/13 06:47 CRDT- 2024/01/31 19:29 PHST- 2023/08/25 00:00 [received] PHST- 2024/01/01 00:00 [revised] PHST- 2024/01/24 00:00 [accepted] PHST- 2024/03/13 06:47 [medline] PHST- 2024/02/01 00:42 [pubmed] PHST- 2024/01/31 19:29 [entrez] AID - S0141-8130(24)00576-2 [pii] AID - 10.1016/j.ijbiomac.2024.129773 [doi] PST - ppublish SO - Int J Biol Macromol. 2024 Mar;261(Pt 2):129773. doi: 10.1016/j.ijbiomac.2024.129773. Epub 2024 Feb 1.