PMID- 38327405
OWN - NLM
STAT- PubMed-not-MEDLINE
LR  - 20240210
IS  - 2405-8440 (Print)
IS  - 2405-8440 (Electronic)
IS  - 2405-8440 (Linking)
VI  - 10
IP  - 3
DP  - 2024 Feb 15
TI  - Synthesis of nano-crystallite hydroxyapatites in different media and a 
      comparative study for estimation of crystallite size using Scherrer method, 
      Halder-Wagner method size-strain plot, and Williamson-Hall model.
PG  - e25347
LID - 10.1016/j.heliyon.2024.e25347 [doi]
LID - e25347
AB  - Hydroxyapatite (HAp) [Ca(10)(PO(4))(6)(OH)(2)] is remarkably similar to the hard 
      tissue of the human body and the uses of this material in various fields in 
      addition to the medical sector are increasing day by day. In this research, 
      mustered oil, soybean oil, as well as coconut oil were employed as liquid media 
      for synthesizing nanocrystalline HAp using a wet chemical precipitation approach. 
      The X-ray diffraction (XRD) study verified the crystalline phase of the HAp in 
      all the indicated media and discovered similarities with the standard database. 
      Several prominent models such as the Scherrer's Method (SM), Halder-Wagner Method 
      (HWM), linear straight-line method (LSLM), Williamson-Hall Method (W-M), Monshi 
      Scherrer Method (MSM), Size-Strain Plot Method (SSPM), Sahadat-Scherrer Method 
      (S-S) were applied for the determination of crystallite size. The stress, strain, 
      and energy density were also computed from the above models. All the models, 
      without the Linear straight-line technique of Scherrer's equation, resulted in an 
      appropriate value of crystallite size for synthesized products. The calculated 
      crystallite sizes were 6.5 nm for HAp in master oil using Halder-Wagner Method, 
      and 143 nm for HAp in coconut oil using the Scherrer equation which were the 
      lowest and the largest, respectively.
CI  - (c) 2024 The Authors.
FAU - Kawsar, Md
AU  - Kawsar M
AD  - Glass Research Division, Institute of Glass & Ceramic Research and Testing, 
      Bangladesh Council of Scientific and Industrial Research (BCSIR), Dhaka-1205, 
      Bangladesh.
AD  - Department of Applied Chemistry and Chemical Engineering, Noakhali Science and 
      Technology University, Noakhali, Bangladesh.
FAU - Hossain, Md Sahadat
AU  - Hossain MS
AD  - Glass Research Division, Institute of Glass & Ceramic Research and Testing, 
      Bangladesh Council of Scientific and Industrial Research (BCSIR), Dhaka-1205, 
      Bangladesh.
FAU - Bahadur, Newaz Mohammed
AU  - Bahadur NM
AD  - Department of Applied Chemistry and Chemical Engineering, Noakhali Science and 
      Technology University, Noakhali, Bangladesh.
FAU - Ahmed, Samina
AU  - Ahmed S
AD  - Glass Research Division, Institute of Glass & Ceramic Research and Testing, 
      Bangladesh Council of Scientific and Industrial Research (BCSIR), Dhaka-1205, 
      Bangladesh.
AD  - BCSIR Dhaka Laboratories, Bangladesh Council of Scientific and Industrial 
      Research (BCSIR), Dhaka-1205, Bangladesh.
LA  - eng
PT  - Journal Article
DEP - 20240130
PL  - England
TA  - Heliyon
JT  - Heliyon
JID - 101672560
PMC - PMC10847954
OTO - NOTNLM
OT  - Crystallite size
OT  - Crystallographic parameter
OT  - Peak profiling
OT  - X-ray diffraction
COIS- The authors declare the following financial interests/personal relationships 
      which may be considered as potential competing interests:There is nothing to 
      declare If there are other authors, they declare that they have no known 
      competing financial interests or personal relationships that could have appeared 
      to influence the work reported in this paper.
EDAT- 2024/02/08 06:42
MHDA- 2024/02/08 06:43
PMCR- 2024/01/30
CRDT- 2024/02/08 04:04
PHST- 2023/09/22 00:00 [received]
PHST- 2024/01/10 00:00 [revised]
PHST- 2024/01/25 00:00 [accepted]
PHST- 2024/02/08 06:43 [medline]
PHST- 2024/02/08 06:42 [pubmed]
PHST- 2024/02/08 04:04 [entrez]
PHST- 2024/01/30 00:00 [pmc-release]
AID - S2405-8440(24)01378-1 [pii]
AID - e25347 [pii]
AID - 10.1016/j.heliyon.2024.e25347 [doi]
PST - epublish
SO  - Heliyon. 2024 Jan 30;10(3):e25347. doi: 10.1016/j.heliyon.2024.e25347. 
      eCollection 2024 Feb 15.