PMID- 38490140
OWN - NLM
STAT- MEDLINE
DCOM- 20240401
LR  - 20240401
IS  - 1873-3778 (Electronic)
IS  - 0021-9673 (Linking)
VI  - 1720
DP  - 2024 Apr 12
TI  - Magnetic polyimide nanocomposite for analysis of parabens in cooking wine by 
      magnetic solid-phase extraction coupled with gas chromatography - Mass 
      spectrometry.
PG  - 464814
LID - S0021-9673(24)00187-0 [pii]
LID - 10.1016/j.chroma.2024.464814 [doi]
AB  - A magnetic polyimide (PI) nanocomposite has been synthesized by phase inversion 
      of PI and simultaneous encapsulation of Fe(3)O(4) nanoparticles. The Fe(3)O(4)/PI 
      nanocomposite was characterized by a variety of characterization techniques, 
      including infrared spectroscopy, scanning electron microscopy, transmission 
      electron microscopy, nitrogen adsorption-desorption isotherms, and vibrating 
      sample magnetometry. The results showed that the prepared nanocomposite had a 
      homogeneous structure, adequate specific surface area (76.1 m(2)/g) and high 
      saturation magnetization (42.9 emu/g). Using parabens as model analytes, the 
      performance of the Fe(3)O(4)/PI nanocomposite as an adsorbent for magnetic 
      solid-phase extraction (MSPE) was evaluated. The extracted parabens were desorbed 
      and determined by gas chromatography-mass spectrometry (GC-MS). The parameters 
      affecting the extraction and desorption efficiency of parabens were optimized. 
      Under the optimal conditions, the developed MSPE/GC-MS method was successfully 
      applied to the determination of parabens in cooking wine. The MSPE/GC-MS method 
      exhibited broad linearity (0.2-100 microg/L), low detection limits (0.04-0.05 microg/L), 
      and satisfactory extraction recoveries (79.2 %-113.3 %) with relative standard 
      deviations (RSDs) ranging from 0.7 % to 10.4 %. For real cooking wine samples, 
      the spiked recoveries ranged from 91.7 % to 118.7 % with RSDs of 1.0 %-11.2 %. 
      The results demonstrated that the Fe(3)O(4)/PI nanocomposite was an effective 
      adsorbent, and this work provides a novel reference for the easy preparation of 
      magnetic adsorbent materials.
CI  - Copyright (c) 2024 Elsevier B.V. All rights reserved.
FAU - Wang, Liuxin
AU  - Wang L
AD  - State Key Laboratory for Managing Biotic and Chemical Threats to the Quality and 
      Safety of Agro-products, State Key Laboratory Base of Novel Functional Materials 
      and Preparation Science, School of Materials Science & Chemical Engineering, 
      Ningbo University, Ningbo, Zhejiang 315211, China.
FAU - Yan, Xiaohui
AU  - Yan X
AD  - State Key Laboratory for Managing Biotic and Chemical Threats to the Quality and 
      Safety of Agro-products, State Key Laboratory Base of Novel Functional Materials 
      and Preparation Science, School of Materials Science & Chemical Engineering, 
      Ningbo University, Ningbo, Zhejiang 315211, China. Electronic address: 
      yanxiaohui@nbu.edu.cn.
FAU - Chen, Xianzhong
AU  - Chen X
AD  - State Key Laboratory for Managing Biotic and Chemical Threats to the Quality and 
      Safety of Agro-products, State Key Laboratory Base of Novel Functional Materials 
      and Preparation Science, School of Materials Science & Chemical Engineering, 
      Ningbo University, Ningbo, Zhejiang 315211, China.
FAU - Li, Yanshuo
AU  - Li Y
AD  - State Key Laboratory for Managing Biotic and Chemical Threats to the Quality and 
      Safety of Agro-products, State Key Laboratory Base of Novel Functional Materials 
      and Preparation Science, School of Materials Science & Chemical Engineering, 
      Ningbo University, Ningbo, Zhejiang 315211, China.
FAU - Wu, Dapeng
AU  - Wu D
AD  - State Key Laboratory for Managing Biotic and Chemical Threats to the Quality and 
      Safety of Agro-products, State Key Laboratory Base of Novel Functional Materials 
      and Preparation Science, School of Materials Science & Chemical Engineering, 
      Ningbo University, Ningbo, Zhejiang 315211, China. Electronic address: 
      wudapeng@nbu.edu.cn.
LA  - eng
PT  - Journal Article
DEP - 20240312
PL  - Netherlands
TA  - J Chromatogr A
JT  - Journal of chromatography. A
JID - 9318488
RN  - 0 (Parabens)
SB  - IM
MH  - Gas Chromatography-Mass Spectrometry
MH  - Parabens
MH  - *Wine
MH  - Adsorption
MH  - Magnetic Phenomena
MH  - Solid Phase Extraction/methods
MH  - *Nanocomposites/chemistry
MH  - Limit of Detection
MH  - Chromatography, High Pressure Liquid/methods
OTO - NOTNLM
OT  - Cooking wine
OT  - Gas chromatography-mass spectrometry
OT  - Magnetic solid-phase extraction
OT  - Parabens
OT  - Polyimide nanocomposite
COIS- Declaration of competing interest The authors declare that they have no known 
      competing financial interests or personal relationships that could have appeared 
      to influence the work reported in this paper.
EDAT- 2024/03/16 05:42
MHDA- 2024/04/01 06:43
CRDT- 2024/03/15 19:13
PHST- 2023/12/16 00:00 [received]
PHST- 2024/03/09 00:00 [revised]
PHST- 2024/03/11 00:00 [accepted]
PHST- 2024/04/01 06:43 [medline]
PHST- 2024/03/16 05:42 [pubmed]
PHST- 2024/03/15 19:13 [entrez]
AID - S0021-9673(24)00187-0 [pii]
AID - 10.1016/j.chroma.2024.464814 [doi]
PST - ppublish
SO  - J Chromatogr A. 2024 Apr 12;1720:464814. doi: 10.1016/j.chroma.2024.464814. Epub 
      2024 Mar 12.