PMID- 38500629
OWN - NLM
STAT- PubMed-not-MEDLINE
LR  - 20240320
IS  - 2046-2069 (Electronic)
IS  - 2046-2069 (Linking)
VI  - 14
IP  - 13
DP  - 2024 Mar 14
TI  - Developing a novel magnetic organic polymer for selective extraction and 
      determination of 16 macrolides in water and honey samples.
PG  - 8726-8734
LID - 10.1039/d4ra00496e [doi]
AB  - A novel magnetic organic polymer Fe(3)O(4)@SiO(2)@Tb-PDAN was designed and 
      synthesized, which was used as an adsorbent for magnetic solid-phase extraction 
      (MSPE) of 16 macrolides (MALs) in water and honey. The synthesized adsorbent was 
      characterized using techniques including scanning electron microscopy (SEM), 
      Fourier transform infrared spectroscopy (FT-IR) and X-ray diffraction (XRD). Then 
      several parameters of the extraction process were further optimized. Under the 
      optimized conditions, an MSPE-LC-MS/MS method was established for extraction and 
      determination of 16 MALs, which showed good linearity (r >/= 0.999), low limits of 
      detection (0.001-0.012 mug L(-1) for water and 0.001-0.367 mug kg(-1) for honey) 
      and satisfactory recoveries (70.02-118.91%) with the relative standard deviations 
      (RSDs) lower than 10.0%. This established method was then successfully applied to 
      detect MALs in real samples, which suggested that Fe(3)O(4)@SiO(2)@Tb-PDAN was a 
      potential magnetic adsorbent for efficient extraction and analysis of MALs.
CI  - This journal is (c) The Royal Society of Chemistry.
FAU - Liang, Mengnan
AU  - Liang M
AD  - College of Chemistry and Materials Science, Hebei Normal University Shijiazhuang 
      050023 China wkecdc@163.com.
FAU - Li, Na
AU  - Li N
AD  - College of Chemistry and Materials Science, Hebei Normal University Shijiazhuang 
      050023 China wkecdc@163.com.
FAU - Zhang, Hao
AU  - Zhang H
AD  - College of Chemistry and Materials Science, Hebei Normal University Shijiazhuang 
      050023 China wkecdc@163.com.
FAU - Ma, Ling
AU  - Ma L
AD  - Shijiazhuang Center for Disease Control and Prevention Shijiazhuang 050011 China 
      mamalin001@163.com.
AD  - Shijiazhuang Technology Innovation Center for Chemical Poison Detection and Risk 
      Early Warning Shijiazhuang 050011 China.
FAU - Wang, Ke
AU  - Wang K
AUID- ORCID: 0000-0003-2117-9786
AD  - College of Chemistry and Materials Science, Hebei Normal University Shijiazhuang 
      050023 China wkecdc@163.com.
AD  - Shijiazhuang Center for Disease Control and Prevention Shijiazhuang 050011 China 
      mamalin001@163.com.
AD  - Shijiazhuang Technology Innovation Center for Chemical Poison Detection and Risk 
      Early Warning Shijiazhuang 050011 China.
LA  - eng
PT  - Journal Article
DEP - 20240318
PL  - England
TA  - RSC Adv
JT  - RSC advances
JID - 101581657
PMC - PMC10945740
COIS- There are no conflicts to declare.
EDAT- 2024/03/19 06:44
MHDA- 2024/03/19 06:45
PMCR- 2024/03/18
CRDT- 2024/03/19 03:37
PHST- 2024/01/19 00:00 [received]
PHST- 2024/03/03 00:00 [accepted]
PHST- 2024/03/19 06:45 [medline]
PHST- 2024/03/19 06:44 [pubmed]
PHST- 2024/03/19 03:37 [entrez]
PHST- 2024/03/18 00:00 [pmc-release]
AID - d4ra00496e [pii]
AID - 10.1039/d4ra00496e [doi]
PST - epublish
SO  - RSC Adv. 2024 Mar 18;14(13):8726-8734. doi: 10.1039/d4ra00496e. eCollection 2024 
      Mar 14.