PMID- 8069120
OWN - NLM
STAT- MEDLINE
DCOM- 19940927
LR  - 20191210
IS  - 1060-3271 (Print)
IS  - 1060-3271 (Linking)
VI  - 77
IP  - 4
DP  - 1994 Jul-Aug
TI  - Liquid chromatographic determination of furazolidone in shrimp.
PG  - 901-4
AB  - A liquid chromatographic (LC) method was developed for the quantitation of 
      furazolidone residues in shrimp muscle. The shrimp homogenate (1.0 g) is 
      extracted with acetonitrile, and the extract is taken to dryness. The residue is 
      dissolved in acetonitrile, and the solution is passed through alumina and C18 
      cleanup columns. The eluate is taken to dryness and reconstituted in a suitable 
      solvent for reversed-phase (C18) LC with UV detection at 365 nm. Recoveries of 
      furazolidone from shrimp homogenates spiked from 5 to 80 ng/g ranged from 74.3 to 
      79.7%, and relative standard deviations (RSDs) were 5.0-8.9%. RSDs for incurred 
      furazolidone quantitated at 5.9 and 9.2 ng/g were 6.6 and 7.6%, respectively.
FAU - Stehly, G R
AU  - Stehly GR
AD  - U.S. Food and Drug Administration, Gulf Coast Seafood Laboratory, Dauphin Island, 
      AL 36528.
FAU - Plakas, S M
AU  - Plakas SM
FAU - el Said, K R
AU  - el Said KR
LA  - eng
PT  - Journal Article
PL  - England
TA  - J AOAC Int
JT  - Journal of AOAC International
JID - 9215446
RN  - 5J9CPU3RE0 (Furazolidone)
SB  - IM
MH  - Animals
MH  - Chromatography, Liquid/*methods
MH  - Decapoda/*chemistry
MH  - Furazolidone/*analysis
EDAT- 1994/07/01 00:00
MHDA- 1994/07/01 00:01
CRDT- 1994/07/01 00:00
PHST- 1994/07/01 00:00 [pubmed]
PHST- 1994/07/01 00:01 [medline]
PHST- 1994/07/01 00:00 [entrez]
PST - ppublish
SO  - J AOAC Int. 1994 Jul-Aug;77(4):901-4.