PMID- 9818413
OWN - NLM
STAT- MEDLINE
DCOM- 19981203
LR  - 20231213
IS  - 0021-9673 (Print)
IS  - 0021-9673 (Linking)
VI  - 823
IP  - 1-2
DP  - 1998 Oct 9
TI  - Determination of polychlorinated biphenyls in soybean infant formulas by gas 
      chromatography.
PG  - 365-72
AB  - A method previously developed for the analysis of organohalogenated compounds in 
      dairy products is now validated for polychlorinated biphenyls (PCBs) 
      determination in soybean infant formulas. The results of this study are 
      consistent with those found for PCBs in powdered full-fat milk. The methodology 
      is based on a solid-liquid extraction step enabling a semi-selective extraction 
      of the apolar lipids of the matrix without affecting the efficiency for the 
      recovery of PCBs. Mean recoveries for the spiked coplanar congeners studied were 
      in the 88-114% range, with relative standard deviations (R.S.D.s) lower than 
      9.8%. The R.S.D.s related to the determination of endogenous PCBs were in the 
      1.5-10.0% range. The validated methodology was applied to the PCB analysis in 
      different trademarks of soybean infant formulas commercialised in Spain. Toxic 
      tetraequivalents of tetrachlorodibenzo-p-dioxin and daily intake corresponding to 
      each one were calculated and compared with values previously published and with 
      those found in literature for human breast milk in different countries.
FAU - Ramos, L
AU  - Ramos L
AD  - Centro de Tecnologia de los Alimentos y Servicios Biosanitarios, Universidad de 
      Alcala, Alcala de Henares, Madrid, Spain.
FAU - Torre, M
AU  - Torre M
FAU - Laborda, F
AU  - Laborda F
FAU - Marina, M L
AU  - Marina ML
LA  - eng
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
PL  - Netherlands
TA  - J Chromatogr A
JT  - Journal of chromatography. A
JID - 9318488
RN  - 0 (Environmental Pollutants)
RN  - DFC2HB4I0K (Polychlorinated Biphenyls)
SB  - IM
MH  - Chromatography, Gas/*methods
MH  - Environmental Pollutants/*analysis
MH  - Humans
MH  - Infant
MH  - Infant Food/*analysis
MH  - Polychlorinated Biphenyls/*analysis/toxicity
MH  - *Glycine max
EDAT- 1998/11/18 00:00
MHDA- 1998/11/18 00:01
CRDT- 1998/11/18 00:00
PHST- 1998/11/18 00:00 [pubmed]
PHST- 1998/11/18 00:01 [medline]
PHST- 1998/11/18 00:00 [entrez]
AID - S0021-9673(98)00514-7 [pii]
AID - 10.1016/s0021-9673(98)00514-7 [doi]
PST - ppublish
SO  - J Chromatogr A. 1998 Oct 9;823(1-2):365-72. doi: 10.1016/s0021-9673(98)00514-7.